mirror of
https://asciireactor.com/otho/phy-4660.git
synced 2024-11-22 18:05:05 +00:00
109 lines
46 KiB
Plaintext
109 lines
46 KiB
Plaintext
|
<?xml version="1.0" encoding="UTF-8"?>
|
||
|
|
<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/1.6" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/1.6 http://www.xrdml.com/XRDMeasurement/1.6/XRDMeasurement.xsd" status="Completed">
|
||
|
|
<comment>
|
||
|
|
<entry>Configuration=Reflection-transmission spinner, Owner=User-1, Creation date=11/29/2016 1:26:51 PM</entry>
|
||
|
|
<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
|
||
|
|
<entry>Sample stage=Reflection-transmission spinner; Minimum step size Phi:0.1</entry>
|
||
|
|
<entry>Diffractometer system=EMPYREAN</entry>
|
||
|
|
<entry>Measurement program=C:\PANalytical\Data Collector\Programs\Burns Cu Spinner Gonio scan zero BH.xrdmp, Identifier={23998444-8D7A-4320-9B40-6587590B817D}</entry>
|
||
|
|
</comment>
|
||
|
|
<sample type="To be analyzed">
|
||
|
|
<id></id>
|
||
|
|
<name></name>
|
||
|
|
<preparedBy></preparedBy>
|
||
|
|
</sample>
|
||
|
|
<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
|
||
|
|
<comment>
|
||
|
|
<entry>PHD Lower Level = 6.52 (keV), PHD Upper Level = 11.27 (keV)</entry>
|
||
|
|
</comment>
|
||
|
|
<usedWavelength intended="K-Alpha 1">
|
||
|
|
<kAlpha1 unit="Angstrom">1.5405980</kAlpha1>
|
||
|
|
<kAlpha2 unit="Angstrom">1.5444260</kAlpha2>
|
||
|
|
<kBeta unit="Angstrom">1.3922500</kBeta>
|
||
|
|
<ratioKAlpha2KAlpha1>0.5000</ratioKAlpha2KAlpha1>
|
||
|
|
</usedWavelength>
|
||
|
|
<incidentBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<xRayTube id="1010048" name="Empyrean Cu LFF HR (9430 033 7310x) DK410577">
|
||
|
|
<tension unit="kV">45.0</tension>
|
||
|
|
<current unit="mA">40.0</current>
|
||
|
|
<anodeMaterial>Cu</anodeMaterial>
|
||
|
|
<focus type="Line">
|
||
|
|
<length unit="mm">12.0</length>
|
||
|
|
<width unit="mm">0.4</width>
|
||
|
|
<takeOffAngle unit="deg">6.0</takeOffAngle>
|
||
|
|
</focus>
|
||
|
|
</xRayTube>
|
||
|
|
<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<mask id="22080002" name="Fixed incident beam mask 10 mm">
|
||
|
|
<distanceToSample unit="mm">100.00</distanceToSample>
|
||
|
|
<width unit="mm">6.60</width>
|
||
|
|
</mask>
|
||
|
|
<antiScatterSlit id="22010003" name="Fixed slit 1°" xsi:type="fixedAntiScatterSlitType">
|
||
|
|
<height unit="mm">1.52</height>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<divergenceSlit id="22010012" name="Programmable divergence slit" xsi:type="automaticDivergenceSlitType">
|
||
|
|
<distanceToSample unit="mm">140.00</distanceToSample>
|
||
|
|
<irradiatedLength unit="mm">5.0</irradiatedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</divergenceSlit>
|
||
|
|
</incidentBeamPath>
|
||
|
|
<sampleMovement xsi:type="spinningSampleMovementType">
|
||
|
|
<spinnerRevolutionTime unit="seconds">2.0</spinnerRevolutionTime>
|
||
|
|
</sampleMovement>
|
||
|
|
<diffractedBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<antiScatterSlit id="22060009" name="Programmable anti-scatter slit" xsi:type="automaticAntiScatterSlitType">
|
||
|
|
<observedLength unit="mm">5.0</observedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<sollerSlit id="21020003" name="Large Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<filter id="20010006" name="Beta-filter Rhodium">
|
||
|
|
<material>Rh</material>
|
||
|
|
<thickness unit="mm">0.050</thickness>
|
||
|
|
</filter>
|
||
|
|
<detector id="7010012" name="X'Celerator Scientific" xsi:type="rtmsDetectorType">
|
||
|
|
<phd>
|
||
|
|
<lowerLevel unit="%">40.5</lowerLevel>
|
||
|
|
<upperLevel unit="%">70.0</upperLevel>
|
||
|
|
</phd>
|
||
|
|
<mode>Scanning</mode>
|
||
|
|
<activeLength unit="deg">2.1223</activeLength>
|
||
|
|
</detector>
|
||
|
|
</diffractedBeamPath>
|
||
|
|
<scan appendNumber="0" mode="Continuous" scanAxis="Gonio" status="Completed">
|
||
|
|
<header>
|
||
|
|
<startTimeStamp>2017-03-30T15:36:39-04:00</startTimeStamp>
|
||
|
|
<endTimeStamp>2017-03-30T15:42:35-04:00</endTimeStamp>
|
||
|
|
<author>
|
||
|
|
<name>User</name>
|
||
|
|
</author>
|
||
|
|
<source>
|
||
|
|
<applicationSoftware version="5.4">Data Collector</applicationSoftware>
|
||
|
|
<instrumentControlSoftware version="7.9d 20161215">EMPYREAN</instrumentControlSoftware>
|
||
|
|
<instrumentID>0000000011187692</instrumentID>
|
||
|
|
</source>
|
||
|
|
</header>
|
||
|
|
<dataPoints>
|
||
|
|
<positions axis="2Theta" unit="deg">
|
||
|
|
<startPosition>5.00547782</startPosition>
|
||
|
|
<endPosition>119.99571965</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Omega" unit="deg">
|
||
|
|
<startPosition>2.50273891</startPosition>
|
||
|
|
<endPosition>59.99785982</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Phi" unit="deg">
|
||
|
|
<commonPosition>0.0</commonPosition>
|
||
|
|
</positions>
|
||
|
|
<commonCountingTime unit="seconds">3.175</commonCountingTime>
|
||
|
|
<intensities unit="counts">47 55 49 41 40 38 47 47 53 44 32 38 49 43 37 42 46 43 56 50 40 32 58 58 31 47 38 52 35 36 35 42 44 54 49 43 35 49 37 56 43 40 48 24 40 47 43 29 37 32 40 41 47 50 41 38 49 49 47 41 42 43 58 47 40 54 44 38 36 46 40 32 27 42 41 42 49 33 47 42 59 36 53 42 29 46 37 29 31 35 52 58 55 53 37 47 55 42 43 38 47 54 31 43 43 40 37 47 50 42 44 48 41 37 56 47 40 43 44 46 53 38 52 56 56 38 35 54 54 43 38 47 48 50 47 35 53 44 41 30 46 58 44 37 42 36 42 61 49 55 37 40 36 30 52 46 40 47 38 36 46 35 38 43 38 40 44 41 58 49 56 42 36 35 38 40 46 33 33 44 46 35 38 42 60 52 35 47 31 54 44 52 67 48 58 38 48 50 43 48 36 40 60 46 40 44 42 48 41 54 76 46 58 47 44 37 44 50 43 43 43 43 37 30 37 40 53 50 38 41 50 41 21 35 36 47 42 42 35 44 44 36 63 44 55 43 54 48 42 44 38 56 37 48 43 52 37 40 35 42 41 36 48 49 44 43 50 41 36 40 42 36 31 55 44 27 35 44 46 33 54 43 49 46 41 58 42 53 50 54 30 48 43 47 38 37 43 53 36 46 55 46 42 52 47 42 30 43 54 40 43 58 33 44 44 38 42 38 42 36 63 33 31 55 36 58 41 30 52 44 48 43 48 48 53 52 54 49 47 49 49 46 25 43 47 53 43 36 40 41 40 41 33 52 53 49 58 48 35 49 42 31 50 36 43 44 35 35 44 54 46 46 41 47 41 35 43 46 32 36 43 43 40 46 46 30 31 44 38 35 41 52 46 42 46 54 49 48 63 54 36 44 44 47 33 38 42 36 55 52 46 42 35 50 47 48 41 42 44 49 42 38 52 42 48 48 52 36 44 52 54 41 41 48 56 40 41 33 46 44 44 77 55 46 41 58 42 40 38 42 54 49 42 44 43 40 42 55 52 49 41 41 37 53 42 49 48 54 31 58 49 40 54 50 35 42 53 43 44 46 50 47 47 40 47 50 54 47 48 38 40 43 32 43 38 52 43 42 40 48 59 48 47 47 44 40 47 36 46 42 40 48 37 43 47 38 41 46 46 50 55 35 32 60 48 50 43 70 41 40 44 46 52 54 35 46 43 37 64 52 55 44 40 46 40 59 52 52 52 25 42 36 43 46 47 48 44 52 55 44 56 46 43 47 48 41 43 41 54 47 60 52 53 38 47 52 47 65 33 52 52 48 36 50 44 60 42 43 37 42 48 49 46 55 50 42 56 56 36 46 47 58 48 50 46 33 56 56 43 33 50 50 41 44 43 58 46 40 37 43 54 44 42 41 29 53 50 46 38 42 54 53 55 42 41 37 40 52 46 44 56 37 42 31 46 37 54 50 37 44 49 40 37 46 54 46 50 50 49 38 44 33 49 50 36 50 47 54 48 60 48 46 67 40 46 44 55 44 47 48 58 33 56 38 42 50 48 42 55 35 53 49 46 61 55 48 48 52 60 52 58 43 43 47 43 53 53 56 41 43 53 47 43 50 38 36 55 44 41 49 41 44 54 35 33 47 41 55 32 55 47 47 46 59 47 43 46 41 60 67 43 36 54 56 33 53 54 40 55 42 27 47 49 55 41 42 49 50 46 44 44 52 32 47 54 42 59 49 33 47 44 47 65 47 47 55 46 58 54 52 60 50 42 47 48 52 43 54 47 44 38 55 59 35 48 55 60 56 40 53 56 58 48 33 48 54 52 54 49 50 52 49 46 58 38 47 53 44 55 47 59 56 58 64 69 55 59 55 73 60 38 40 52 63 40 58 50 43 47 41 49 54 50 54 43 54 55 44 58 59 64 55 49 44 64 43 33 58 53 58 38 55 55 63 44 53 58 59 50 54 63 59 61 54 49 52 50 54 54 50 69 56 53 47 66 50 54 49 48 60 70 64 41 61 55 24 48 48 38 47 52 58 58 56 64 63 56 47 70 59 52 59 37 60 53 44 61 61 59 48 49 43 50 41 58 63 49 52 61 63 69 46 60 55 58 38 49 60 67 47 48 49 49 77 50 42 52 55 49 50 56 41 55 47 44 49 61 50 54 47 47 53 50 47 48 59 56 46 38 70 54 61 50 54 69 33 56 56 48 42 56 56 56 46 44 58 50 50 61 59 54 58 49 43 52 63 50 54 56 49 58 56 53 64 58 49 50 48 54 52 44 56 54 63 54 63 43 58 52 50 44 61 43 54 59 44 49 47 55 46 50 41 55 58 61 46 49 60 48 44 48 47 44 54 53 52 63 52 53 54 67 52 52 54 52 43 50 50 43 46 49 55 50 48 49 56 55 60 56 49 37 48 48 69 54 63 46 48 44 52 76 41 44 52 50 46 43 55 71 49 49 63 41 55 61 65 67 56 56 52 53 64 60 54 58 55 54 55 50 58 64 60 60 61 49 54 53 50 44 71 49 71 52 56 60 47 42 36 41 52 67 61 43 49 54 59 52 60 52 53 44 66 54 61 43 61 54 66 46 63 65 47 49 43 60 54 50 52 59 47 64 49 41 47 58 52 67 52 50 56 59 49 59 49 56 49 50 53 48 46 59 50 72 52 63 66 47 52 47 56 36 54 52 48 73 55 43 41 64 43 56 63 52 54 52 64 67 58 59 55 47 44 63 63 61 60 67 52 54 50 61 59 56 64 61 52 44 49 44 71 63 55 44 50 60 46 35 53 60 49 53 52 56 54 52 53 54 59 48 55 55 67 48 64 44 50 48 59 55 46 70 55 58 48 58 59 50 59 55 49 50 49 61 52 54 63 41 46 48 59 50 55 61 49 53 58 50 64 48 56 49 47 52 58 58 61 63 65 38 58 63 54 47 50 52 52 49 60 61 53 56 38 50 49 54 64 48 37 59 38 48 65 46 56 55 56 47 47 46 47 43 52 58 72 46 67 58 46 54 49 71 50 48 53 42 46 41 48 52 54 48 59 65 43 56
|
||
|
|
</dataPoints>
|
||
|
|
</scan>
|
||
|
|
</xrdMeasurement>
|
||
|
|
</xrdMeasurements>
|