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109 lines
46 KiB
Plaintext
109 lines
46 KiB
Plaintext
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<?xml version="1.0" encoding="UTF-8"?>
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<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/1.6" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/1.6 http://www.xrdml.com/XRDMeasurement/1.6/XRDMeasurement.xsd" status="Completed">
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<comment>
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<entry>Configuration=Reflection-transmission spinner, Owner=User-1, Creation date=11/29/2016 1:26:51 PM</entry>
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<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
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<entry>Sample stage=Reflection-transmission spinner; Minimum step size Phi:0.1</entry>
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<entry>Diffractometer system=EMPYREAN</entry>
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<entry>Measurement program=C:\PANalytical\Data Collector\Programs\Burns Cu Spinner Gonio scan zero BH.xrdmp, Identifier={23998444-8D7A-4320-9B40-6587590B817D}</entry>
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</comment>
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<sample type="To be analyzed">
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<id></id>
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<name></name>
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<preparedBy></preparedBy>
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</sample>
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<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
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<comment>
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<entry>PHD Lower Level = 6.52 (keV), PHD Upper Level = 11.27 (keV)</entry>
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</comment>
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<usedWavelength intended="K-Alpha 1">
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<kAlpha1 unit="Angstrom">1.5405980</kAlpha1>
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<kAlpha2 unit="Angstrom">1.5444260</kAlpha2>
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<kBeta unit="Angstrom">1.3922500</kBeta>
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<ratioKAlpha2KAlpha1>0.5000</ratioKAlpha2KAlpha1>
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</usedWavelength>
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<incidentBeamPath>
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<radius unit="mm">240.00</radius>
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<xRayTube id="1010048" name="Empyrean Cu LFF HR (9430 033 7310x) DK410577">
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<tension unit="kV">45.0</tension>
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<current unit="mA">40.0</current>
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<anodeMaterial>Cu</anodeMaterial>
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<focus type="Line">
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<length unit="mm">12.0</length>
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<width unit="mm">0.4</width>
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<takeOffAngle unit="deg">6.0</takeOffAngle>
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</focus>
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</xRayTube>
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<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
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<opening unit="rad">0.0400</opening>
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</sollerSlit>
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<mask id="22080002" name="Fixed incident beam mask 10 mm">
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<distanceToSample unit="mm">100.00</distanceToSample>
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<width unit="mm">6.60</width>
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</mask>
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<antiScatterSlit id="22010003" name="Fixed slit 1°" xsi:type="fixedAntiScatterSlitType">
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<height unit="mm">1.52</height>
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</antiScatterSlit>
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<divergenceSlit id="22010012" name="Programmable divergence slit" xsi:type="automaticDivergenceSlitType">
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<distanceToSample unit="mm">140.00</distanceToSample>
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<irradiatedLength unit="mm">5.0</irradiatedLength>
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<offset unit="mm">0.00</offset>
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</divergenceSlit>
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</incidentBeamPath>
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<sampleMovement xsi:type="spinningSampleMovementType">
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<spinnerRevolutionTime unit="seconds">2.0</spinnerRevolutionTime>
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</sampleMovement>
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<diffractedBeamPath>
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<radius unit="mm">240.00</radius>
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<antiScatterSlit id="22060009" name="Programmable anti-scatter slit" xsi:type="automaticAntiScatterSlitType">
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<observedLength unit="mm">5.0</observedLength>
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<offset unit="mm">0.00</offset>
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</antiScatterSlit>
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<sollerSlit id="21020003" name="Large Soller slits 0.04 rad.">
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<opening unit="rad">0.0400</opening>
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</sollerSlit>
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<filter id="20010006" name="Beta-filter Rhodium">
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<material>Rh</material>
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<thickness unit="mm">0.050</thickness>
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</filter>
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<detector id="7010012" name="X'Celerator Scientific" xsi:type="rtmsDetectorType">
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<phd>
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<lowerLevel unit="%">40.5</lowerLevel>
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<upperLevel unit="%">70.0</upperLevel>
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</phd>
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<mode>Scanning</mode>
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<activeLength unit="deg">2.1223</activeLength>
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</detector>
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</diffractedBeamPath>
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<scan appendNumber="0" mode="Continuous" scanAxis="Gonio" status="Completed">
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<header>
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<startTimeStamp>2017-03-30T15:02:24-04:00</startTimeStamp>
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<endTimeStamp>2017-03-30T15:08:22-04:00</endTimeStamp>
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<author>
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<name>User</name>
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</author>
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<source>
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<applicationSoftware version="5.4">Data Collector</applicationSoftware>
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<instrumentControlSoftware version="7.9d 20161215">EMPYREAN</instrumentControlSoftware>
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<instrumentID>0000000011187692</instrumentID>
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</source>
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</header>
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<dataPoints>
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<positions axis="2Theta" unit="deg">
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<startPosition>5.00547782</startPosition>
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<endPosition>119.99571965</endPosition>
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</positions>
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<positions axis="Omega" unit="deg">
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<startPosition>2.50273891</startPosition>
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<endPosition>59.99785982</endPosition>
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</positions>
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<positions axis="Phi" unit="deg">
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<commonPosition>0.0</commonPosition>
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</positions>
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<commonCountingTime unit="seconds">3.175</commonCountingTime>
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<intensities unit="counts">23 30 40 15 32 25 35 37 35 36 25 49 40 41 31 37 37 20 36 38 40 23 36 42 33 30 36 38 36 21 33 35 46 52 35 30 36 31 19 33 27 35 44 37 33 29 31 42 37 47 40 43 40 32 44 41 29 31 31 26 35 38 33 32 27 25 30 27 32 49 35 41 35 37 40 41 49 55 41 24 31 26 33 50 30 36 33 33 40 40 35 37 36 42 38 37 36 44 40 32 33 32 37 50 44 36 40 44 46 30 29 36 41 37 43 50 48 26 43 36 40 41 32 36 38 32 26 46 36 37 49 32 49 53 53 26 35 42 40 43 21 25 36 37 50 38 38 41 40 42 38 31 37 43 37 31 40 27 37 41 55 32 40 33 29 40 36 33 36 44 40 49 29 43 37 40 53 32 41 43 38 35 43 41 42 41 41 43 38 46 43 36 43 44 38 35 44 48 43 53 55 42 53 47 40 56 37 41 37 37 37 37 35 26 24 36 38 37 41 47 50 32 47 29 41 49 44 46 43 46 48 37 33 40 40 40 43 33 49 46 42 38 46 37 43 36 50 46 35 43 49 36 48 41 41 40 46 40 42 35 42 41 30 58 35 54 46 55 36 41 27 41 26 54 40 47 41 32 43 52 55 43 43 42 46 38 32 47 40 44 26 37 42 58 38 49 41 40 46 43 40 38 48 48 31 36 31 44 50 35 43 41 58 49 32 54 53 35 59 44 43 41 31 50 43 33 37 50 48 40 55 44 47 41 43 37 47 37 32 40 35 37 29 53 40 38 47 58 55 38 35 46 41 61 49 47 47 41 41 44 52 46 55 41 54 44 41 44 42 36 48 40 43 59 50 48 56 56 44 38 35 52 52 47 49 70 42 41 32 52 40 40 43 43 48 36 50 49 42 60 44 36 46 44 27 52 43 42 49 46 37 66 66 43 47 38 42 43 42 58 30 41 47 42 33 41 46 50 44 53 47 50 53 43 47 43 36 47 43 44 47 54 55 50 53 33 44 38 37 26 36 46 49 54 44 52 61 43 46 43 33 32 44 50 56 44 41 41 52 52 48 54 43 48 52 47 37 43 56 44 55 65 53 55 48 48 32 35 56 53 42 48 54 46 48 58 48 53 43 60 42 56 38 49 53 42 49 50 40 53 46 46 46 37 41 53 36 48 37 44 49 56 52 44 40 52 60 49 40 58 50 42 48 46 41 42 48 48 44 46 44 47 48 43 44 54 49 44 54 38 53 48 44 33 41 55 54 52 54 41 55 56 44 35 54 63 46 41 64 53 58 59 46 50 47 49 26 46 49 52 48 50 64 49 40 48 41 48 40 48 58 40 38 44 53 44 54 50 44 41 49 55 42 38 53 50 54 50 47 40 65 50 52 33 33 71 46 48 47 50 58 44 47 38 50 44 59 46 46 64 38 59 47 47 52 47 53 59 42 48 48 33 53 40 60 30 48 48 52 48 47 49 54 53 59 47 63 30 65 52 43 54 65 50 60 53 52 60 50 55 46 67 44 41 54 49 33 49 61 50 69 52 54 58 52 42 36 44 55 59 43 40 54 43 47 50 52 42 46 49 46 41 52 52 59 47 65 55 54 63 69 42 58 49 56 56 41 44 55 54 46 47 46 42 61 48 43 47 42 44 48 55 67 44 52 43 44 36 31 61 48 54 49 61 37 53 50 64 63 36 61 61 44 60 41 56 43 58 44 47 42 36 56 46 56 42 48 47 63 32 43 56 49 43 58 61 56 41 42 60 49 60 43 47 47 52 44 53 46 38 42 58 44 47 55 52 41 59 36 50 58 44 48 43 56 59 42 65 48 53 47 66 42 50 59 53 48 42 59 59 41 41 44 52 38 71 52 46 53 56 44 47 61 58 41 60 61 56 49 58 52 38 50 54 52 58 49 56 48 50 44 43 55 55 47 48 60 42 54 61 53 44 46 48 50 48 54 49 52 46 54 46 60 60 36 64 54 46 35 47 47 64 31 38 56 60 58 60 48 44 53 44 60 49 54 58 52 41 50 44 55 55 41 50 66 49 58 59 44 54 56 53 50 46 67 49 47 58 63 55 60 65 55 60 71 44 38 64 53 50 58 49 48 55 53 49 52 44 65 46 63 44 43 71 46 58 54 63 61 54 59 52 63 61 54 52 48 47 55 35 49 50 52 50 55 61 44 52 54 50 44 61 52 43 58 54 49 54 49 46 48 42 37 43 53 53 63 60 59 48 41 66 60 55 47 43 49 38 48 40 63 55 48 56 54 47 64 41 61 47 56 44 52 47 43 48 55 60 50 48 52 52 53 44 56 47 47 63 50 56 48 48 48 44 56 56 58 48 59 46 55 53 52 47 44 50 46 52 48 53 60 52 38 37 49 49 56 41 50 54 53 58 50 60 46 54 49 58 52 60 46 55 54 47 46 59 54 49 54 61 70 41 52 50 56 56 48 37 53 38 55 52 49 56 29 48 60 55 50 48 55 55 54 58 35 48 63 50 43 49 58 41 49 48 52 46 56 58 55 48 59 69 47 48 43 43 49 42 46 32 38 36 56 43 61 63 46 60 42 53 60 53 48 43 53 54 53 43 53 63 48 38 33 48 49 41 49 48 73 38 43 47 50 37 52 44 61 52 50 65 59 44 42 52 55 60 58 46 36 49 40 41 58 53 41 46 43 42 54 44 46 52 50 56 41 52 49 52 60 49 44 48 42 63 48 52 52 50 41 43 58 48 44 44 40 56 54 54 53 42 52 48 56 67 46 60 50 49 50 54 49 58 44 40 53 53 56 47 48 43 53 42 50 48 35 48 54 48 59 43 55 48 53 54 37 48 32 59 43 44 44 47 67 52 55 43 41 54 46 56 55 53 56 55 58 42 53 38 53 47 48 47 56 47 52 44 41 53 53 46 50 46 37 47 49 46 46 36 41 47 44 54 54 49 44 54 43 48 43 49 46 52 56 41 49 52 58 52 53 49 53 44 44 59 50 43 41 47 37 50 50 64 42 42 48 48 32 49 56 47 48 49 43 44 50 54 44 55 44 54 43 44 61 63 42
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</dataPoints>
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</scan>
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</xrdMeasurement>
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</xrdMeasurements>
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