mirror of
https://asciireactor.com/otho/phy-4660.git
synced 2024-11-22 16:05:07 +00:00
109 lines
50 KiB
Plaintext
109 lines
50 KiB
Plaintext
|
<?xml version="1.0" encoding="UTF-8"?>
|
||
|
|
<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/1.6" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/1.6 http://www.xrdml.com/XRDMeasurement/1.6/XRDMeasurement.xsd" status="Completed">
|
||
|
|
<comment>
|
||
|
|
<entry>Configuration=Reflection-transmission spinner, Owner=User-1, Creation date=11/29/2016 1:26:51 PM</entry>
|
||
|
|
<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
|
||
|
|
<entry>Sample stage=Reflection-transmission spinner; Minimum step size Phi:0.1</entry>
|
||
|
|
<entry>Diffractometer system=EMPYREAN</entry>
|
||
|
|
<entry>Measurement program=C:\PANalytical\Data Collector\Programs\Burns Cu Spinner Gonio scan zero BH.xrdmp, Identifier={23998444-8D7A-4320-9B40-6587590B817D}</entry>
|
||
|
|
</comment>
|
||
|
|
<sample type="To be analyzed">
|
||
|
|
<id></id>
|
||
|
|
<name></name>
|
||
|
|
<preparedBy></preparedBy>
|
||
|
|
</sample>
|
||
|
|
<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
|
||
|
|
<comment>
|
||
|
|
<entry>PHD Lower Level = 6.52 (keV), PHD Upper Level = 11.27 (keV)</entry>
|
||
|
|
</comment>
|
||
|
|
<usedWavelength intended="K-Alpha 1">
|
||
|
|
<kAlpha1 unit="Angstrom">1.5405980</kAlpha1>
|
||
|
|
<kAlpha2 unit="Angstrom">1.5444260</kAlpha2>
|
||
|
|
<kBeta unit="Angstrom">1.3922500</kBeta>
|
||
|
|
<ratioKAlpha2KAlpha1>0.5000</ratioKAlpha2KAlpha1>
|
||
|
|
</usedWavelength>
|
||
|
|
<incidentBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<xRayTube id="1010048" name="Empyrean Cu LFF HR (9430 033 7310x) DK410577">
|
||
|
|
<tension unit="kV">45.0</tension>
|
||
|
|
<current unit="mA">40.0</current>
|
||
|
|
<anodeMaterial>Cu</anodeMaterial>
|
||
|
|
<focus type="Line">
|
||
|
|
<length unit="mm">12.0</length>
|
||
|
|
<width unit="mm">0.4</width>
|
||
|
|
<takeOffAngle unit="deg">6.0</takeOffAngle>
|
||
|
|
</focus>
|
||
|
|
</xRayTube>
|
||
|
|
<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<mask id="22080002" name="Fixed incident beam mask 10 mm">
|
||
|
|
<distanceToSample unit="mm">100.00</distanceToSample>
|
||
|
|
<width unit="mm">6.60</width>
|
||
|
|
</mask>
|
||
|
|
<antiScatterSlit id="22010003" name="Fixed slit 1°" xsi:type="fixedAntiScatterSlitType">
|
||
|
|
<height unit="mm">1.52</height>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<divergenceSlit id="22010012" name="Programmable divergence slit" xsi:type="automaticDivergenceSlitType">
|
||
|
|
<distanceToSample unit="mm">140.00</distanceToSample>
|
||
|
|
<irradiatedLength unit="mm">5.0</irradiatedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</divergenceSlit>
|
||
|
|
</incidentBeamPath>
|
||
|
|
<sampleMovement xsi:type="spinningSampleMovementType">
|
||
|
|
<spinnerRevolutionTime unit="seconds">2.0</spinnerRevolutionTime>
|
||
|
|
</sampleMovement>
|
||
|
|
<diffractedBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<antiScatterSlit id="22060009" name="Programmable anti-scatter slit" xsi:type="automaticAntiScatterSlitType">
|
||
|
|
<observedLength unit="mm">5.0</observedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<sollerSlit id="21020003" name="Large Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<filter id="20010006" name="Beta-filter Rhodium">
|
||
|
|
<material>Rh</material>
|
||
|
|
<thickness unit="mm">0.050</thickness>
|
||
|
|
</filter>
|
||
|
|
<detector id="7010012" name="X'Celerator Scientific" xsi:type="rtmsDetectorType">
|
||
|
|
<phd>
|
||
|
|
<lowerLevel unit="%">40.5</lowerLevel>
|
||
|
|
<upperLevel unit="%">70.0</upperLevel>
|
||
|
|
</phd>
|
||
|
|
<mode>Scanning</mode>
|
||
|
|
<activeLength unit="deg">2.1223</activeLength>
|
||
|
|
</detector>
|
||
|
|
</diffractedBeamPath>
|
||
|
|
<scan appendNumber="0" mode="Continuous" scanAxis="Gonio" status="Completed">
|
||
|
|
<header>
|
||
|
|
<startTimeStamp>2017-03-30T16:05:37-04:00</startTimeStamp>
|
||
|
|
<endTimeStamp>2017-03-30T16:11:36-04:00</endTimeStamp>
|
||
|
|
<author>
|
||
|
|
<name>User</name>
|
||
|
|
</author>
|
||
|
|
<source>
|
||
|
|
<applicationSoftware version="5.4">Data Collector</applicationSoftware>
|
||
|
|
<instrumentControlSoftware version="7.9d 20161215">EMPYREAN</instrumentControlSoftware>
|
||
|
|
<instrumentID>0000000011187692</instrumentID>
|
||
|
|
</source>
|
||
|
|
</header>
|
||
|
|
<dataPoints>
|
||
|
|
<positions axis="2Theta" unit="deg">
|
||
|
|
<startPosition>5.00547782</startPosition>
|
||
|
|
<endPosition>119.99571965</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Omega" unit="deg">
|
||
|
|
<startPosition>2.50273891</startPosition>
|
||
|
|
<endPosition>59.99785982</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Phi" unit="deg">
|
||
|
|
<commonPosition>0.0</commonPosition>
|
||
|
|
</positions>
|
||
|
|
<commonCountingTime unit="seconds">3.175</commonCountingTime>
|
||
|
|
<intensities unit="counts">25 41 35 50 37 44 32 43 33 31 43 42 40 33 38 53 31 47 40 49 49 43 37 48 38 32 36 50 58 38 35 36 35 53 46 32 42 36 47 37 40 46 31 53 49 41 33 33 46 43 35 44 52 42 36 48 40 44 65 40 46 61 47 30 32 48 32 44 46 37 46 46 55 41 54 35 44 47 27 42 53 53 40 35 33 41 42 43 50 55 37 46 50 30 43 53 53 49 44 40 44 41 49 48 65 46 46 56 47 37 43 61 40 56 35 41 59 35 37 49 33 31 48 37 33 41 50 53 48 54 49 32 43 32 55 49 52 40 50 56 58 43 40 32 44 60 40 59 43 40 52 32 41 46 58 53 36 43 44 43 50 55 53 44 43 42 46 47 46 40 52 36 48 43 43 53 47 38 43 46 35 42 42 48 55 50 43 52 38 44 47 43 47 64 63 55 54 49 55 61 47 46 41 69 42 48 42 38 50 29 54 38 50 47 50 46 46 55 55 49 53 37 48 32 46 44 43 40 54 63 36 50 48 41 43 42 53 59 47 49 42 56 46 35 53 54 56 47 46 46 46 37 37 48 47 55 55 40 27 32 56 43 35 42 32 42 47 43 52 61 47 55 46 55 42 50 56 49 59 37 47 42 48 55 60 42 40 48 53 37 44 48 47 48 46 60 56 69 58 44 49 43 49 46 65 42 55 36 55 44 47 38 38 53 66 55 43 53 67 53 54 48 49 43 54 50 44 41 50 47 44 49 47 52 61 41 37 47 50 60 64 65 54 47 53 58 59 48 53 36 52 58 43 61 43 42 38 43 52 66 49 55 46 47 71 71 38 49 56 49 35 46 44 48 49 41 46 59 52 52 50 60 49 52 55 54 60 41 58 47 54 59 48 63 56 66 38 46 49 59 48 50 49 38 36 46 40 70 63 52 67 54 63 44 55 56 43 44 80 47 43 64 41 43 66 50 59 66 46 63 40 54 46 55 64 54 50 53 56 53 40 60 53 61 46 50 49 61 70 38 58 44 61 54 46 55 64 38 36 47 47 61 49 47 58 65 41 64 55 49 48 52 52 43 44 52 50 40 63 58 50 43 56 53 48 49 53 64 35 49 44 44 66 54 49 63 52 50 44 73 38 52 63 66 38 41 48 53 38 58 58 55 60 60 47 49 64 47 67 56 56 58 40 50 52 69 54 55 58 47 60 56 49 44 52 64 49 50 59 64 53 66 43 48 60 52 47 55 55 49 73 66 50 66 65 65 44 46 69 56 65 58 70 50 53 70 52 60 44 49 66 48 47 44 48 59 43 60 54 44 61 52 54 56 48 55 56 47 54 61 66 50 48 55 48 61 52 49 48 52 73 76 55 49 52 52 53 41 47 54 56 52 67 63 54 54 63 61 54 56 53 58 48 53 54 49 55 50 58 60 70 30 53 47 54 50 54 64 54 49 58 63 52 64 47 49 54 58 72 71 50 61 66 58 60 72 48 40 43 53 55 75 46 63 42 43 50 50 56 44 71 66 52 54 52 41 49 50 64 58 73 48 75 43 54 82 54 56 53 60 61 61 54 55 60 61 50 50 53 63 58 77 47 53 67 61 42 55 54 70 59 69 55 54 71 50 60 59 54 58 48 58 46 48 72 61 65 47 69 58 69 56 75 65 54 71 40 44 67 48 69 52 66 53 77 58 58 48 69 64 40 60 65 43 70 53 52 58 69 59 44 58 64 53 59 60 56 59 67 78 58 71 48 60 61 55 65 55 48 54 60 63 53 59 54 50 71 63 59 69 58 59 53 67 69 56 59 48 65 72 55 55 56 70 72 60 64 61 50 56 50 55 63 53 53 53 52 55 59 56 63 73 56 60 60 55 52 66 44 63 75 63 70 52 54 63 56 60 67 41 71 73 52 66 59 66 61 46 54 70 61 50 72 67 65 44 42 50 60 73 61 55 58 72 73 63 42 58 69 66 54 60 75 52 66 61 60 64 52 93 55 64 60 61 66 64 69 61 55 52 69 48 61 66 61 54 54 49 42 52 50 64 67 58 72 50 59 67 77 69 65 61 59 55 53 55 67 54 56 64 77 64 78 59 49 56 47 59 60 66 53 73 56 67 53 53 50 49 67 49 48 52 47 61 60 65 56 54 69 70 56 55 59 49 58 82 53 69 53 63 55 64 56 66 52 52 67 56 59 65 75 80 65 76 77 65 77 63 53 58 61 65 56 69 55 48 60 61 70 77 61 64 67 60 59 73 50 69 76 59 66 42 70 71 54 65 54 58 53 61 65 58 71 67 70 66 67 73 63 49 71 77 76 55 70 56 55 71 67 70 49 42 77 76 66 71 60 56 53 61 87 65 76 63 65 56 59 53 61 63 81 69 70 58 52 53 73 59 65 80 55 60 52 53 66 55 59 61 69 56 65 75 71 56 67 63 59 78 64 70 69 63 54 83 70 58 78 73 73 65 67 70 64 58 73 70 50 78 59 70 61 70 55 55 63 59 48 67 61 73 70 60 67 76 65 66 58 55 72 54 61 64 60 61 78 72 63 78 60 65 73 63 69 72 70 70 88 58 67 65 71 81 78 64 71 67 77 59 71 67 67 50 61 58 69 72 70 58 84 78 70 78 72 72 70 82 66 72 69 81 58 71 81 61 93 82 67 75 58 75 83 67 96 65 69 72 76 72 86 78 83 61 75 69 75 69 67 83 58 60 73 72 75 70 76 78 66 88 75 56 58 82 83 77 50 50 75 50 75 78 61 87 80 71 77 71 87 66 75 69 77 66 60 70 64 82 67 59 92 75 82 89 70 58 58 70 67 67 66 71 67 69 64 61 73 60 72 83 75 60 78 63 61 80 73 77 83 76 71 61 47 84 77 80 78 67 75 90 83 58 67 83 73 66 59 70 89 93 87 72 67 56 88 75 54 63 83 63 83 70 92 78 77 81 81 70 72 90 81 84 80 78 56 80 83 65 80 86 73 82 75 72 93 73 82 86 66 77 64 77 73 88 83 78 94 71 86 77 95 66 67 88 72 84 81 83 84 89 94 72 76 67 86 87 94
|
||
|
|
</dataPoints>
|
||
|
|
</scan>
|
||
|
|
</xrdMeasurement>
|
||
|
|
</xrdMeasurements>
|