mirror of
https://asciireactor.com/otho/phy-4660.git
synced 2024-11-25 11:15:05 +00:00
109 lines
52 KiB
Plaintext
109 lines
52 KiB
Plaintext
|
<?xml version="1.0" encoding="UTF-8"?>
|
||
|
|
<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/1.6" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/1.6 http://www.xrdml.com/XRDMeasurement/1.6/XRDMeasurement.xsd" status="Completed">
|
||
|
|
<comment>
|
||
|
|
<entry>Configuration=Reflection-transmission spinner, Owner=User-1, Creation date=11/29/2016 1:26:51 PM</entry>
|
||
|
|
<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
|
||
|
|
<entry>Sample stage=Reflection-transmission spinner; Minimum step size Phi:0.1</entry>
|
||
|
|
<entry>Diffractometer system=EMPYREAN</entry>
|
||
|
|
<entry>Measurement program=C:\PANalytical\Data Collector\Programs\Burns Cu Spinner Gonio scan zero BH.xrdmp, Identifier={23998444-8D7A-4320-9B40-6587590B817D}</entry>
|
||
|
|
</comment>
|
||
|
|
<sample type="To be analyzed">
|
||
|
|
<id></id>
|
||
|
|
<name></name>
|
||
|
|
<preparedBy></preparedBy>
|
||
|
|
</sample>
|
||
|
|
<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
|
||
|
|
<comment>
|
||
|
|
<entry>PHD Lower Level = 6.52 (keV), PHD Upper Level = 11.27 (keV)</entry>
|
||
|
|
</comment>
|
||
|
|
<usedWavelength intended="K-Alpha 1">
|
||
|
|
<kAlpha1 unit="Angstrom">1.5405980</kAlpha1>
|
||
|
|
<kAlpha2 unit="Angstrom">1.5444260</kAlpha2>
|
||
|
|
<kBeta unit="Angstrom">1.3922500</kBeta>
|
||
|
|
<ratioKAlpha2KAlpha1>0.5000</ratioKAlpha2KAlpha1>
|
||
|
|
</usedWavelength>
|
||
|
|
<incidentBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<xRayTube id="1010048" name="Empyrean Cu LFF HR (9430 033 7310x) DK410577">
|
||
|
|
<tension unit="kV">45.0</tension>
|
||
|
|
<current unit="mA">40.0</current>
|
||
|
|
<anodeMaterial>Cu</anodeMaterial>
|
||
|
|
<focus type="Line">
|
||
|
|
<length unit="mm">12.0</length>
|
||
|
|
<width unit="mm">0.4</width>
|
||
|
|
<takeOffAngle unit="deg">6.0</takeOffAngle>
|
||
|
|
</focus>
|
||
|
|
</xRayTube>
|
||
|
|
<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<mask id="22080002" name="Fixed incident beam mask 10 mm">
|
||
|
|
<distanceToSample unit="mm">100.00</distanceToSample>
|
||
|
|
<width unit="mm">6.60</width>
|
||
|
|
</mask>
|
||
|
|
<antiScatterSlit id="22010003" name="Fixed slit 1°" xsi:type="fixedAntiScatterSlitType">
|
||
|
|
<height unit="mm">1.52</height>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<divergenceSlit id="22010012" name="Programmable divergence slit" xsi:type="automaticDivergenceSlitType">
|
||
|
|
<distanceToSample unit="mm">140.00</distanceToSample>
|
||
|
|
<irradiatedLength unit="mm">5.0</irradiatedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</divergenceSlit>
|
||
|
|
</incidentBeamPath>
|
||
|
|
<sampleMovement xsi:type="spinningSampleMovementType">
|
||
|
|
<spinnerRevolutionTime unit="seconds">2.0</spinnerRevolutionTime>
|
||
|
|
</sampleMovement>
|
||
|
|
<diffractedBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<antiScatterSlit id="22060009" name="Programmable anti-scatter slit" xsi:type="automaticAntiScatterSlitType">
|
||
|
|
<observedLength unit="mm">5.0</observedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<sollerSlit id="21020003" name="Large Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<filter id="20010006" name="Beta-filter Rhodium">
|
||
|
|
<material>Rh</material>
|
||
|
|
<thickness unit="mm">0.050</thickness>
|
||
|
|
</filter>
|
||
|
|
<detector id="7010012" name="X'Celerator Scientific" xsi:type="rtmsDetectorType">
|
||
|
|
<phd>
|
||
|
|
<lowerLevel unit="%">40.5</lowerLevel>
|
||
|
|
<upperLevel unit="%">70.0</upperLevel>
|
||
|
|
</phd>
|
||
|
|
<mode>Scanning</mode>
|
||
|
|
<activeLength unit="deg">2.1223</activeLength>
|
||
|
|
</detector>
|
||
|
|
</diffractedBeamPath>
|
||
|
|
<scan appendNumber="0" mode="Continuous" scanAxis="Gonio" status="Completed">
|
||
|
|
<header>
|
||
|
|
<startTimeStamp>2017-03-30T16:22:45-04:00</startTimeStamp>
|
||
|
|
<endTimeStamp>2017-03-30T16:28:42-04:00</endTimeStamp>
|
||
|
|
<author>
|
||
|
|
<name>User</name>
|
||
|
|
</author>
|
||
|
|
<source>
|
||
|
|
<applicationSoftware version="5.4">Data Collector</applicationSoftware>
|
||
|
|
<instrumentControlSoftware version="7.9d 20161215">EMPYREAN</instrumentControlSoftware>
|
||
|
|
<instrumentID>0000000011187692</instrumentID>
|
||
|
|
</source>
|
||
|
|
</header>
|
||
|
|
<dataPoints>
|
||
|
|
<positions axis="2Theta" unit="deg">
|
||
|
|
<startPosition>5.00547782</startPosition>
|
||
|
|
<endPosition>119.99571965</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Omega" unit="deg">
|
||
|
|
<startPosition>2.50273891</startPosition>
|
||
|
|
<endPosition>59.99785982</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Phi" unit="deg">
|
||
|
|
<commonPosition>0.0</commonPosition>
|
||
|
|
</positions>
|
||
|
|
<commonCountingTime unit="seconds">3.175</commonCountingTime>
|
||
|
|
<intensities unit="counts">65 54 52 50 53 67 41 67 50 66 67 63 46 47 67 72 73 67 69 61 50 49 66 67 60 58 63 69 58 59 58 61 69 61 61 80 58 67 47 65 64 58 54 46 50 61 56 61 55 55 66 59 54 63 60 71 58 58 63 60 66 54 67 58 56 61 67 67 63 53 56 67 70 59 64 78 71 67 64 70 70 66 75 70 44 64 61 89 49 65 67 77 72 54 55 66 60 56 56 59 64 60 78 77 67 64 72 83 50 54 76 70 60 63 60 69 67 61 72 63 56 56 50 60 61 66 72 61 54 81 66 70 65 59 69 63 56 84 63 72 64 63 83 69 54 65 70 70 70 63 58 73 64 78 71 67 75 71 61 71 71 64 56 78 78 73 70 89 67 71 58 64 76 76 72 75 65 71 77 53 67 60 58 66 69 72 76 78 65 65 78 75 75 67 67 70 75 65 72 77 77 73 67 75 88 66 53 69 67 70 72 75 63 72 78 56 75 65 65 69 72 75 87 66 78 71 60 92 58 76 71 67 65 66 77 77 70 80 92 56 66 81 78 66 87 77 72 80 69 80 66 86 66 83 81 77 77 84 67 66 67 73 81 80 92 65 76 75 65 72 87 78 80 76 87 73 75 78 53 84 81 59 82 84 59 77 86 76 86 81 75 89 86 87 103 67 83 88 87 71 78 84 86 87 71 99 64 90 78 93 83 96 76 94 96 92 88 75 76 83 96 75 60 70 83 76 76 81 109 87 99 76 76 81 75 92 100 69 77 55 82 109 89 86 76 96 88 84 78 90 77 81 87 75 103 93 95 116 86 96 89 106 86 95 98 88 95 81 100 95 93 103 88 88 96 107 100 78 86 84 70 88 76 100 99 87 88 81 99 96 76 104 96 99 82 96 86 103 96 92 93 106 96 109 93 81 98 83 98 86 75 87 84 120 116 96 110 98 86 88 75 93 93 88 105 78 103 107 109 90 90 89 94 103 89 99 93 120 106 101 127 109 81 89 105 112 111 107 126 87 111 106 112 103 84 124 121 111 143 122 105 113 117 113 117 128 117 101 120 103 96 127 86 103 117 101 105 105 120 98 127 103 120 103 99 126 128 94 94 133 112 110 129 115 112 121 113 117 101 135 141 109 107 124 121 115 134 112 115 93 126 94 118 132 133 120 134 120 113 118 150 155 124 109 132 163 107 128 123 144 124 156 118 139 146 145 130 156 138 139 127 149 127 128 145 104 103 139 143 147 145 144 147 135 144 150 152 147 149 140 155 146 172 133 186 150 140 145 128 144 126 174 144 169 132 161 167 132 149 156 129 161 140 153 156 178 168 170 173 152 168 174 170 156 153 181 144 169 175 173 176 180 185 175 153 187 166 157 167 169 180 175 161 160 170 158 206 173 176 195 189 210 183 210 180 178 180 176 198 167 197 202 207 208 206 169 230 227 166 190 201 189 191 190 196 202 176 225 192 218 193 226 226 176 216 192 202 202 204 193 224 189 197 233 219 195 215 200 201 216 210 220 200 233 225 229 231 212 261 208 207 241 200 233 215 232 280 218 233 246 196 204 224 243 248 249 249 233 231 254 233 252 252 277 242 277 238 258 231 247 238 255 226 242 244 237 273 278 271 259 260 283 260 266 263 250 243 281 283 258 253 226 246 269 267 265 242 260 303 264 270 275 315 269 299 288 269 316 266 267 264 270 278 295 335 278 277 298 290 288 283 290 273 306 306 306 280 328 305 293 295 313 295 306 310 267 289 335 267 300 305 299 295 311 322 300 294 298 264 260 301 292 298 280 330 310 286 320 258 276 292 316 310 299 322 297 288 284 293 347 300 312 332 295 311 346 345 298 299 267 298 324 329 326 288 293 320 292 311 315 301 309 306 318 338 305 313 283 322 337 312 299 352 311 311 337 284 282 293 305 328 301 329 294 338 337 298 320 326 326 295 320 300 293 339 295 283 305 281 288 349 289 301 289 335 323 323 306 272 299 288 332 301 289 330 317 294 287 278 305 298 313 289 275 294 306 298 306 289 297 264 310 264 271 281 289 275 277 273 295 277 303 301 300 278 300 298 261 303 273 266 280 284 272 235 292 293 286 263 276 305 261 267 261 263 282 244 290 263 243 299 287 266 263 290 263 286 270 263 264 248 286 272 275 288 259 278 277 259 281 242 289 272 231 264 250 269 306 275 264 221 253 267 235 231 276 284 276 271 236 283 236 238 226 266 229 260 271 236 233 233 236 241 231 243 215 254 261 242 254 248 233 207 235 238 283 240 235 233 214 292 221 223 255 247 225 227 264 215 226 220 224 238 240 248 242 249 243 246 238 215 220 261 210 200 243 244 220 224 257 261 206 215 215 246 220 225 196 224 233 212 246 227 229 243 241 247 229 213 212 233 225 258 201 259 240 248 224 238 225 210 221 241 221 219 215 206 240 192 226 203 218 198 204 224 218 218 253 232 207 207 207 232 203 214 207 238 208 226 223 243 230 223 213 224 198 213 223 221 226 189 213 202 242 219 213 196 195 224 196 221 215 1
|
||
|
|
</dataPoints>
|
||
|
|
</scan>
|
||
|
|
</xrdMeasurement>
|
||
|
|
</xrdMeasurements>
|