mirror of
https://asciireactor.com/otho/phy-4660.git
synced 2024-11-22 15:55:07 +00:00
109 lines
59 KiB
Plaintext
109 lines
59 KiB
Plaintext
|
<?xml version="1.0" encoding="UTF-8"?>
|
||
|
<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/1.6" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/1.6 http://www.xrdml.com/XRDMeasurement/1.6/XRDMeasurement.xsd" status="Completed">
|
||
|
<comment>
|
||
|
<entry>Configuration=Reflection-transmission spinner, Owner=User-1, Creation date=11/29/2016 1:26:51 PM</entry>
|
||
|
<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
|
||
|
<entry>Sample stage=Reflection-transmission spinner; Minimum step size Phi:0.1</entry>
|
||
|
<entry>Diffractometer system=EMPYREAN</entry>
|
||
|
<entry>Measurement program=C:\PANalytical\Data Collector\Programs\Burns Cu Spinner Gonio scan zero BH.xrdmp, Identifier={23998444-8D7A-4320-9B40-6587590B817D}</entry>
|
||
|
</comment>
|
||
|
<sample type="To be analyzed">
|
||
|
<id></id>
|
||
|
<name></name>
|
||
|
<preparedBy></preparedBy>
|
||
|
</sample>
|
||
|
<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
|
||
|
<comment>
|
||
|
<entry>PHD Lower Level = 6.52 (keV), PHD Upper Level = 11.27 (keV)</entry>
|
||
|
</comment>
|
||
|
<usedWavelength intended="K-Alpha 1">
|
||
|
<kAlpha1 unit="Angstrom">1.5405980</kAlpha1>
|
||
|
<kAlpha2 unit="Angstrom">1.5444260</kAlpha2>
|
||
|
<kBeta unit="Angstrom">1.3922500</kBeta>
|
||
|
<ratioKAlpha2KAlpha1>0.5000</ratioKAlpha2KAlpha1>
|
||
|
</usedWavelength>
|
||
|
<incidentBeamPath>
|
||
|
<radius unit="mm">240.00</radius>
|
||
|
<xRayTube id="1010048" name="Empyrean Cu LFF HR (9430 033 7310x) DK410577">
|
||
|
<tension unit="kV">45.0</tension>
|
||
|
<current unit="mA">40.0</current>
|
||
|
<anodeMaterial>Cu</anodeMaterial>
|
||
|
<focus type="Line">
|
||
|
<length unit="mm">12.0</length>
|
||
|
<width unit="mm">0.4</width>
|
||
|
<takeOffAngle unit="deg">6.0</takeOffAngle>
|
||
|
</focus>
|
||
|
</xRayTube>
|
||
|
<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
|
||
|
<opening unit="rad">0.0400</opening>
|
||
|
</sollerSlit>
|
||
|
<mask id="22080002" name="Fixed incident beam mask 10 mm">
|
||
|
<distanceToSample unit="mm">100.00</distanceToSample>
|
||
|
<width unit="mm">6.60</width>
|
||
|
</mask>
|
||
|
<antiScatterSlit id="22010003" name="Fixed slit 1°" xsi:type="fixedAntiScatterSlitType">
|
||
|
<height unit="mm">1.52</height>
|
||
|
</antiScatterSlit>
|
||
|
<divergenceSlit id="22010012" name="Programmable divergence slit" xsi:type="automaticDivergenceSlitType">
|
||
|
<distanceToSample unit="mm">140.00</distanceToSample>
|
||
|
<irradiatedLength unit="mm">5.0</irradiatedLength>
|
||
|
<offset unit="mm">0.00</offset>
|
||
|
</divergenceSlit>
|
||
|
</incidentBeamPath>
|
||
|
<sampleMovement xsi:type="spinningSampleMovementType">
|
||
|
<spinnerRevolutionTime unit="seconds">2.0</spinnerRevolutionTime>
|
||
|
</sampleMovement>
|
||
|
<diffractedBeamPath>
|
||
|
<radius unit="mm">240.00</radius>
|
||
|
<antiScatterSlit id="22060009" name="Programmable anti-scatter slit" xsi:type="automaticAntiScatterSlitType">
|
||
|
<observedLength unit="mm">5.0</observedLength>
|
||
|
<offset unit="mm">0.00</offset>
|
||
|
</antiScatterSlit>
|
||
|
<sollerSlit id="21020003" name="Large Soller slits 0.04 rad.">
|
||
|
<opening unit="rad">0.0400</opening>
|
||
|
</sollerSlit>
|
||
|
<filter id="20010006" name="Beta-filter Rhodium">
|
||
|
<material>Rh</material>
|
||
|
<thickness unit="mm">0.050</thickness>
|
||
|
</filter>
|
||
|
<detector id="7010012" name="X'Celerator Scientific" xsi:type="rtmsDetectorType">
|
||
|
<phd>
|
||
|
<lowerLevel unit="%">40.5</lowerLevel>
|
||
|
<upperLevel unit="%">70.0</upperLevel>
|
||
|
</phd>
|
||
|
<mode>Scanning</mode>
|
||
|
<activeLength unit="deg">2.1223</activeLength>
|
||
|
</detector>
|
||
|
</diffractedBeamPath>
|
||
|
<scan appendNumber="0" mode="Continuous" scanAxis="Gonio" status="Completed">
|
||
|
<header>
|
||
|
<startTimeStamp>2017-03-30T16:31:17-04:00</startTimeStamp>
|
||
|
<endTimeStamp>2017-03-30T16:37:13-04:00</endTimeStamp>
|
||
|
<author>
|
||
|
<name>User</name>
|
||
|
</author>
|
||
|
<source>
|
||
|
<applicationSoftware version="5.4">Data Collector</applicationSoftware>
|
||
|
<instrumentControlSoftware version="7.9d 20161215">EMPYREAN</instrumentControlSoftware>
|
||
|
<instrumentID>0000000011187692</instrumentID>
|
||
|
</source>
|
||
|
</header>
|
||
|
<dataPoints>
|
||
|
<positions axis="2Theta" unit="deg">
|
||
|
<startPosition>5.00547782</startPosition>
|
||
|
<endPosition>119.99571965</endPosition>
|
||
|
</positions>
|
||
|
<positions axis="Omega" unit="deg">
|
||
|
<startPosition>2.50273891</startPosition>
|
||
|
<endPosition>59.99785982</endPosition>
|
||
|
</positions>
|
||
|
<positions axis="Phi" unit="deg">
|
||
|
<commonPosition>0.0</commonPosition>
|
||
|
</positions>
|
||
|
<commonCountingTime unit="seconds">3.175</commonCountingTime>
|
||
|
<intensities unit="counts">80 70 78 86 93 65 87 83 89 81 101 93 92 82 86 77 77 88 89 77 92 93 86 70 83 77 84 86 96 81 105 94 83 71 92 67 86 89 89 83 88 75 98 81 90 99 71 76 73 70 99 81 86 87 98 73 98 98 104 88 99 75 99 100 82 88 78 92 93 88 87 105 81 89 89 84 82 93 92 96 107 94 106 104 100 95 115 93 101 88 80 81 90 99 84 93 117 89 67 82 90 93 105 93 93 77 88 111 98 110 95 106 99 118 87 99 96 109 104 81 88 105 92 105 113 89 110 113 104 101 109 104 109 113 99 111 105 104 78 80 107 111 94 86 99 113 89 106 103 117 118 111 84 98 116 109 112 94 98 123 105 105 126 93 140 89 86 104 115 90 112 101 104 105 103 112 111 96 135 115 130 96 89 110 110 112 95 133 123 111 95 84 106 87 117 120 110 132 124 116 105 104 128 122 101 118 99 93 127 115 121 110 107 130 128 122 124 118 124 115 104 132 110 120 104 124 133 124 120 123 128 126 129 117 152 117 123 133 106 116 127 113 90 110 107 138 121 113 115 121 117 110 116 122 135 116 118 127 138 103 115 113 113 135 126 134 126 101 138 135 112 100 111 115 155 107 144 112 126 113 106 129 122 128 144 128 141 136 123 126 121 138 143 130 126 134 140 127 147 134 112 149 132 129 129 149 128 128 123 147 149 153 103 139 134 138 160 134 130 133 134 133 135 128 136 130 128 161 139 136 134 143 167 132 135 122 155 162 158 149 168 144 113 143 128 146 153 139 152 145 139 143 120 155 139 170 145 134 156 150 140 164 163 123 156 155 134 168 151 163 136 134 145 145 149 187 160 147 135 163 140 162 162 163 155 175 162 144 147 149 147 173 167 129 140 167 162 124 145 169 146 173 179 163 169 172 166 180 141 149 151 155 163 155 161 164 141 174 157 151 140 144 160 146 169 162 153 155 163 176 168 173 191 203 169 172 150 173 155 189 146 153 170 170 152 195 157 176 178 175 166 183 169 180 156 147 166 183 178 191 155 179 176 186 186 176 196 192 164 181 166 161 193 146 169 201 189 161 176 158 193 170 179 169 207 175 169 184 168 168 197 158 176 164 181 198 191 161 184 191 200 173 174 185 180 190 203 196 176 186 175 189 186 209 170 196 173 173 198 193 193 162 200 180 207 184 181 192 198 203 163 201 201 196 203 193 163 204 200 184 184 191 187 203 209 230 214 233 223 189 195 200 184 196 207 202 201 214 221 197 178 200 170 203 180 202 240 201 208 187 208 208 241 200 214 203 189 189 195 214 191 163 204 215 233 230 204 218 210 176 180 221 209 220 218 235 213 227 212 240 231 207 224 231 250 219 212 230 225 226 218 200 216 210 201 229 203 223 210 229 193 240 244 221 221 219 210 218 210 219 230 255 210 266 226 229 215 201 272 218 223 208 220 202 215 207 218 265 244 231 215 210 201 259 226 252 207 223 235 248 198 230 227 243 197 219 218 235 232 231 241 253 207 216 243 231 230 219 276 226 223 232 253 265 260 277 240 273 255 235 259 254 219 246 292 246 232 231 257 248 258 229 254 254 247 230 249 264 226 248 280 269 242 226 221 250 269 221 241 272 254 238 301 276 250 244 243 241 223 281 265 278 244 237 272 249 264 271 244 304 265 242 264 283 278 267 282 270 259 273 269 266 286 271 238 275 289 273 290 277 259 305 281 278 259 265 253 276 257 272 289 263 304 298 267 261 258 260 246 267 255 271 287 249 277 300 290 261 270 295 303 272 295 292 286 263 294 261 276 288 280 289 282 282 299 306 294 290 313 293 318 321 303 315 289 284 300 301 292 307 280 283 324 281 306 326 313 287 330 299 311 304 305 320 317 338 289 321 266 321 299 310 298 323 327 323 326 330 315 323 335 305 313 294 310 328 309 305 337 326 338 372 328 295 304 313 306 326 327 330 344 310 335 301 341 328 387 328 349 351 352 344 345 305 335 367 298 366 330 338 377 367 350 340 341 333 357 323 384 396 349 352 375 377 341 377 364 432 395 360 345 357 374 380 418 386 412 401 386 373 374 364 386 370 397 432 391 393 403 407 444 367 425 396 426 397 414 421 410 408 379 430 400 402 396 418 386 402 471 419 407 404 457 415 414 463 472 437 430 433 447 403 461 425 429 459 459 459 444 407 443 459 438 430 429 465 440 459 482 463 449 466 478 453 482 436 486 464 554 492 454 499 472 480 505 481 494 470 518 495 493 501 501 528 566 492 499 521 520 528 556 518 551 490 514 510 544 529 552 534 503 527 554 509 567 552 563 573 552 526 517 541 579 573 583 558 567 537 547 577 578 606 574 586 579 562 596 598 5
|
||
|
</dataPoints>
|
||
|
</scan>
|
||
|
</xrdMeasurement>
|
||
|
</xrdMeasurements>
|