mirror of
https://asciireactor.com/otho/phy-4660.git
synced 2024-11-23 00:55:06 +00:00
109 lines
48 KiB
Plaintext
109 lines
48 KiB
Plaintext
|
<?xml version="1.0" encoding="UTF-8"?>
|
||
|
<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/1.6" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/1.6 http://www.xrdml.com/XRDMeasurement/1.6/XRDMeasurement.xsd" status="Completed">
|
||
|
<comment>
|
||
|
<entry>Configuration=Reflection-transmission spinner, Owner=User-1, Creation date=11/29/2016 1:26:51 PM</entry>
|
||
|
<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
|
||
|
<entry>Sample stage=Reflection-transmission spinner; Minimum step size Phi:0.1</entry>
|
||
|
<entry>Diffractometer system=EMPYREAN</entry>
|
||
|
<entry>Measurement program=C:\PANalytical\Data Collector\Programs\Burns Cu Spinner Gonio scan zero BH.xrdmp, Identifier={23998444-8D7A-4320-9B40-6587590B817D}</entry>
|
||
|
</comment>
|
||
|
<sample type="To be analyzed">
|
||
|
<id></id>
|
||
|
<name></name>
|
||
|
<preparedBy></preparedBy>
|
||
|
</sample>
|
||
|
<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
|
||
|
<comment>
|
||
|
<entry>PHD Lower Level = 6.52 (keV), PHD Upper Level = 11.27 (keV)</entry>
|
||
|
</comment>
|
||
|
<usedWavelength intended="K-Alpha 1">
|
||
|
<kAlpha1 unit="Angstrom">1.5405980</kAlpha1>
|
||
|
<kAlpha2 unit="Angstrom">1.5444260</kAlpha2>
|
||
|
<kBeta unit="Angstrom">1.3922500</kBeta>
|
||
|
<ratioKAlpha2KAlpha1>0.5000</ratioKAlpha2KAlpha1>
|
||
|
</usedWavelength>
|
||
|
<incidentBeamPath>
|
||
|
<radius unit="mm">240.00</radius>
|
||
|
<xRayTube id="1010048" name="Empyrean Cu LFF HR (9430 033 7310x) DK410577">
|
||
|
<tension unit="kV">45.0</tension>
|
||
|
<current unit="mA">40.0</current>
|
||
|
<anodeMaterial>Cu</anodeMaterial>
|
||
|
<focus type="Line">
|
||
|
<length unit="mm">12.0</length>
|
||
|
<width unit="mm">0.4</width>
|
||
|
<takeOffAngle unit="deg">6.0</takeOffAngle>
|
||
|
</focus>
|
||
|
</xRayTube>
|
||
|
<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
|
||
|
<opening unit="rad">0.0400</opening>
|
||
|
</sollerSlit>
|
||
|
<mask id="22080002" name="Fixed incident beam mask 10 mm">
|
||
|
<distanceToSample unit="mm">100.00</distanceToSample>
|
||
|
<width unit="mm">6.60</width>
|
||
|
</mask>
|
||
|
<antiScatterSlit id="22010003" name="Fixed slit 1°" xsi:type="fixedAntiScatterSlitType">
|
||
|
<height unit="mm">1.52</height>
|
||
|
</antiScatterSlit>
|
||
|
<divergenceSlit id="22010012" name="Programmable divergence slit" xsi:type="automaticDivergenceSlitType">
|
||
|
<distanceToSample unit="mm">140.00</distanceToSample>
|
||
|
<irradiatedLength unit="mm">5.0</irradiatedLength>
|
||
|
<offset unit="mm">0.00</offset>
|
||
|
</divergenceSlit>
|
||
|
</incidentBeamPath>
|
||
|
<sampleMovement xsi:type="spinningSampleMovementType">
|
||
|
<spinnerRevolutionTime unit="seconds">2.0</spinnerRevolutionTime>
|
||
|
</sampleMovement>
|
||
|
<diffractedBeamPath>
|
||
|
<radius unit="mm">240.00</radius>
|
||
|
<antiScatterSlit id="22060009" name="Programmable anti-scatter slit" xsi:type="automaticAntiScatterSlitType">
|
||
|
<observedLength unit="mm">5.0</observedLength>
|
||
|
<offset unit="mm">0.00</offset>
|
||
|
</antiScatterSlit>
|
||
|
<sollerSlit id="21020003" name="Large Soller slits 0.04 rad.">
|
||
|
<opening unit="rad">0.0400</opening>
|
||
|
</sollerSlit>
|
||
|
<filter id="20010006" name="Beta-filter Rhodium">
|
||
|
<material>Rh</material>
|
||
|
<thickness unit="mm">0.050</thickness>
|
||
|
</filter>
|
||
|
<detector id="7010012" name="X'Celerator Scientific" xsi:type="rtmsDetectorType">
|
||
|
<phd>
|
||
|
<lowerLevel unit="%">40.5</lowerLevel>
|
||
|
<upperLevel unit="%">70.0</upperLevel>
|
||
|
</phd>
|
||
|
<mode>Scanning</mode>
|
||
|
<activeLength unit="deg">2.1223</activeLength>
|
||
|
</detector>
|
||
|
</diffractedBeamPath>
|
||
|
<scan appendNumber="0" mode="Continuous" scanAxis="Gonio" status="Completed">
|
||
|
<header>
|
||
|
<startTimeStamp>2017-03-30T16:42:54-04:00</startTimeStamp>
|
||
|
<endTimeStamp>2017-03-30T16:48:53-04:00</endTimeStamp>
|
||
|
<author>
|
||
|
<name>User</name>
|
||
|
</author>
|
||
|
<source>
|
||
|
<applicationSoftware version="5.4">Data Collector</applicationSoftware>
|
||
|
<instrumentControlSoftware version="7.9d 20161215">EMPYREAN</instrumentControlSoftware>
|
||
|
<instrumentID>0000000011187692</instrumentID>
|
||
|
</source>
|
||
|
</header>
|
||
|
<dataPoints>
|
||
|
<positions axis="2Theta" unit="deg">
|
||
|
<startPosition>5.00547782</startPosition>
|
||
|
<endPosition>119.99571965</endPosition>
|
||
|
</positions>
|
||
|
<positions axis="Omega" unit="deg">
|
||
|
<startPosition>2.50273891</startPosition>
|
||
|
<endPosition>59.99785982</endPosition>
|
||
|
</positions>
|
||
|
<positions axis="Phi" unit="deg">
|
||
|
<commonPosition>0.0</commonPosition>
|
||
|
</positions>
|
||
|
<commonCountingTime unit="seconds">3.175</commonCountingTime>
|
||
|
<intensities unit="counts">56 35 43 36 43 43 58 31 32 44 40 32 43 32 36 42 40 46 29 41 40 30 29 46 32 38 33 41 40 33 31 33 33 44 40 36 47 35 44 47 37 50 35 38 42 32 33 41 53 46 50 27 44 40 50 41 40 54 41 54 47 31 41 29 46 42 37 46 44 48 31 54 40 44 42 52 44 55 42 43 33 48 48 49 43 52 54 54 40 35 44 48 35 56 50 50 55 42 41 33 46 58 44 33 43 41 49 42 35 54 47 50 46 46 37 36 50 49 46 58 47 25 44 41 41 48 37 56 41 36 52 43 40 55 49 50 42 44 47 44 33 48 30 44 41 47 41 50 53 46 46 44 53 48 48 41 36 48 48 41 50 53 53 32 38 43 44 40 53 66 59 40 31 46 37 42 46 46 41 46 43 54 64 50 52 54 42 44 37 46 46 50 64 47 50 49 48 66 43 42 48 50 53 43 46 47 56 47 46 54 50 53 55 38 49 44 46 54 60 40 54 49 55 48 48 41 38 50 61 40 56 56 38 41 54 52 48 48 48 60 47 46 63 46 58 48 43 60 50 47 55 61 59 55 53 53 36 33 46 49 47 38 54 43 53 52 44 43 47 54 61 53 47 42 43 58 49 47 33 60 47 60 72 44 53 43 60 50 52 58 40 32 47 46 54 60 38 37 53 56 50 70 65 44 49 52 42 53 40 59 63 52 59 42 65 48 54 50 61 53 48 40 64 52 58 70 58 56 44 47 53 59 52 60 66 52 67 47 56 46 41 56 54 66 50 55 59 50 49 58 48 69 63 46 42 61 47 56 38 55 56 69 63 70 52 58 46 55 50 48 37 49 49 58 44 52 44 46 58 50 59 37 54 48 60 43 41 59 60 48 48 61 46 46 54 52 54 64 37 63 52 49 38 47 58 43 42 63 50 63 36 52 52 43 52 54 52 53 59 52 55 42 58 61 60 50 40 48 54 58 65 53 52 46 50 64 55 55 55 40 58 63 43 61 55 56 69 35 56 48 42 59 58 56 49 47 52 54 47 49 43 65 49 70 43 58 44 54 58 43 61 58 48 52 53 47 50 59 36 41 42 49 65 48 54 53 61 65 43 44 48 43 49 52 60 67 58 48 53 50 58 50 55 55 38 41 64 50 47 55 58 37 50 63 49 56 58 42 66 55 53 53 38 54 73 63 60 46 42 52 56 61 66 55 64 70 52 59 64 36 50 53 48 48 71 55 50 52 52 52 71 47 53 52 35 46 44 58 55 48 64 64 58 53 55 53 60 56 56 46 50 56 61 41 78 76 49 41 69 67 50 48 70 63 54 64 66 58 55 64 53 56 58 54 67 48 47 55 50 49 56 53 43 63 54 58 53 49 44 38 52 49 52 56 64 48 58 53 50 61 56 54 55 52 54 49 55 61 44 47 61 38 63 56 41 52 58 46 56 63 53 60 59 49 66 64 70 52 53 50 47 55 56 55 56 54 64 54 58 37 49 66 61 53 53 55 44 55 69 77 55 73 67 46 71 55 56 49 59 44 71 66 54 59 46 58 49 56 63 53 55 66 76 60 59 49 69 56 72 50 60 60 50 63 61 55 52 64 58 65 54 44 60 66 46 63 58 59 66 59 55 63 46 76 66 55 49 64 61 71 48 46 63 49 50 70 50 44 60 43 65 63 49 59 46 73 56 69 56 63 55 64 54 50 44 61 46 60 38 63 60 40 54 65 69 47 72 59 55 61 55 55 58 54 55 50 61 60 56 66 65 59 64 64 60 65 53 60 64 56 49 42 56 56 64 46 66 60 58 50 71 72 59 67 44 55 61 73 67 73 72 58 71 73 52 53 52 61 52 55 70 49 54 59 61 72 52 41 60 65 60 54 66 61 49 56 64 48 59 61 66 58 55 65 46 64 76 61 59 65 41 59 56 65 64 56 58 64 77 71 60 52 63 49 64 73 46 60 64 67 53 63 56 63 59 66 55 48 61 77 66 56 75 67 69 64 71 73 66 65 71 58 56 63 53 61 59 66 64 55 47 55 58 50 65 83 90 69 48 55 67 63 82 47 72 59 70 54 52 55 67 56 60 59 48 55 59 76 69 63 72 59 53 70 55 54 46 53 83 52 54 82 54 61 67 58 58 81 70 56 66 70 70 60 56 53 80 52 48 59 71 72 64 73 71 80 58 58 72 55 71 69 55 65 63 58 76 59 64 47 67 78 50 59 75 60 66 65 66 60 82 69 63 48 59 58 72 73 72 72 65 72 69 63 65 82 55 78 69 55 72 64 66 65 86 64 67 70 63 60 69 61 64 76 73 63 77 66 63 61 78 66 72 60 65 64 69 71 73 71 55 78 66 56 83 77 77 64 98 55 76 67 73 65 78 76 59 70 64 58 61 53 61 49 81 73 70 65 69 88 52 82 67 72 61 63 77 83 75 75 59 60 52 77 63 90 82 59 80 81 80 56 77 69 66 84 76 76 59 67 69 77 71 89 71 71 70 76 64 67 76 61 81 67 63 75 80 69 75 67 69 63 86 71 66 84 73 70 84 66 80 76 82 77 73 72 92 55 84 72 83 81 80 82 77 95 56 83 83 104 90 81 89 76 76 81 66 71 86 64 82 95 72 83 71 71 92 94 76 90 82 63 84 77 73 83 88 89 84 84 87 72 72 73 83 55 78 71 99 99 87 89 65 77 81 72 71 86 94 80 87 92 69 77 94 89 84 87 86 75 75 87 65 101 87 82 92 86 92 101 72 84 93 83 83 82 99 87 83 87 78 83 72 66 92 99 73 80 76 104 86 95 94 83 76 90 93 84 101 98 86 100 126 99 83 71 95 86 96 92 96 96 87 90 78 92 93 115 83 92 98 100 92 92 78 112 98 95 77 86 83 101 96 69 99 101 99 84 95 98 82 81 101 89 96 96 99 94 110 98 80 99 103 112 82 89 88 88 112 122 82 81 95 94 93 110 110 105 105 89 94 90 95 98 89 107 89 100 100 96 89 106 93 113 111 98 104 95 86 103 101 106 94 107
|
||
|
</dataPoints>
|
||
|
</scan>
|
||
|
</xrdMeasurement>
|
||
|
</xrdMeasurements>
|