mirror of
https://asciireactor.com/otho/phy-4660.git
synced 2024-11-25 05:15:08 +00:00
109 lines
59 KiB
Plaintext
109 lines
59 KiB
Plaintext
|
<?xml version="1.0" encoding="UTF-8"?>
|
||
|
|
<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/1.6" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/1.6 http://www.xrdml.com/XRDMeasurement/1.6/XRDMeasurement.xsd" status="Completed">
|
||
|
|
<comment>
|
||
|
|
<entry>Configuration=Reflection-transmission spinner, Owner=User-1, Creation date=11/29/2016 1:26:51 PM</entry>
|
||
|
|
<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
|
||
|
|
<entry>Sample stage=Reflection-transmission spinner; Minimum step size Phi:0.1</entry>
|
||
|
|
<entry>Diffractometer system=EMPYREAN</entry>
|
||
|
|
<entry>Measurement program=C:\PANalytical\Data Collector\Programs\Burns Cu Spinner Gonio scan zero BH.xrdmp, Identifier={23998444-8D7A-4320-9B40-6587590B817D}</entry>
|
||
|
|
</comment>
|
||
|
|
<sample type="To be analyzed">
|
||
|
|
<id></id>
|
||
|
|
<name></name>
|
||
|
|
<preparedBy></preparedBy>
|
||
|
|
</sample>
|
||
|
|
<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
|
||
|
|
<comment>
|
||
|
|
<entry>PHD Lower Level = 6.52 (keV), PHD Upper Level = 11.27 (keV)</entry>
|
||
|
|
</comment>
|
||
|
|
<usedWavelength intended="K-Alpha 1">
|
||
|
|
<kAlpha1 unit="Angstrom">1.5405980</kAlpha1>
|
||
|
|
<kAlpha2 unit="Angstrom">1.5444260</kAlpha2>
|
||
|
|
<kBeta unit="Angstrom">1.3922500</kBeta>
|
||
|
|
<ratioKAlpha2KAlpha1>0.5000</ratioKAlpha2KAlpha1>
|
||
|
|
</usedWavelength>
|
||
|
|
<incidentBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<xRayTube id="1010048" name="Empyrean Cu LFF HR (9430 033 7310x) DK410577">
|
||
|
|
<tension unit="kV">45.0</tension>
|
||
|
|
<current unit="mA">40.0</current>
|
||
|
|
<anodeMaterial>Cu</anodeMaterial>
|
||
|
|
<focus type="Line">
|
||
|
|
<length unit="mm">12.0</length>
|
||
|
|
<width unit="mm">0.4</width>
|
||
|
|
<takeOffAngle unit="deg">6.0</takeOffAngle>
|
||
|
|
</focus>
|
||
|
|
</xRayTube>
|
||
|
|
<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<mask id="22080002" name="Fixed incident beam mask 10 mm">
|
||
|
|
<distanceToSample unit="mm">100.00</distanceToSample>
|
||
|
|
<width unit="mm">6.60</width>
|
||
|
|
</mask>
|
||
|
|
<antiScatterSlit id="22010003" name="Fixed slit 1°" xsi:type="fixedAntiScatterSlitType">
|
||
|
|
<height unit="mm">1.52</height>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<divergenceSlit id="22010012" name="Programmable divergence slit" xsi:type="automaticDivergenceSlitType">
|
||
|
|
<distanceToSample unit="mm">140.00</distanceToSample>
|
||
|
|
<irradiatedLength unit="mm">5.0</irradiatedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</divergenceSlit>
|
||
|
|
</incidentBeamPath>
|
||
|
|
<sampleMovement xsi:type="spinningSampleMovementType">
|
||
|
|
<spinnerRevolutionTime unit="seconds">2.0</spinnerRevolutionTime>
|
||
|
|
</sampleMovement>
|
||
|
|
<diffractedBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<antiScatterSlit id="22060009" name="Programmable anti-scatter slit" xsi:type="automaticAntiScatterSlitType">
|
||
|
|
<observedLength unit="mm">5.0</observedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<sollerSlit id="21020003" name="Large Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<filter id="20010006" name="Beta-filter Rhodium">
|
||
|
|
<material>Rh</material>
|
||
|
|
<thickness unit="mm">0.050</thickness>
|
||
|
|
</filter>
|
||
|
|
<detector id="7010012" name="X'Celerator Scientific" xsi:type="rtmsDetectorType">
|
||
|
|
<phd>
|
||
|
|
<lowerLevel unit="%">40.5</lowerLevel>
|
||
|
|
<upperLevel unit="%">70.0</upperLevel>
|
||
|
|
</phd>
|
||
|
|
<mode>Scanning</mode>
|
||
|
|
<activeLength unit="deg">2.1223</activeLength>
|
||
|
|
</detector>
|
||
|
|
</diffractedBeamPath>
|
||
|
|
<scan appendNumber="0" mode="Continuous" scanAxis="Gonio" status="Completed">
|
||
|
|
<header>
|
||
|
|
<startTimeStamp>2017-03-30T15:27:45-04:00</startTimeStamp>
|
||
|
|
<endTimeStamp>2017-03-30T15:33:44-04:00</endTimeStamp>
|
||
|
|
<author>
|
||
|
|
<name>User</name>
|
||
|
|
</author>
|
||
|
|
<source>
|
||
|
|
<applicationSoftware version="5.4">Data Collector</applicationSoftware>
|
||
|
|
<instrumentControlSoftware version="7.9d 20161215">EMPYREAN</instrumentControlSoftware>
|
||
|
|
<instrumentID>0000000011187692</instrumentID>
|
||
|
|
</source>
|
||
|
|
</header>
|
||
|
|
<dataPoints>
|
||
|
|
<positions axis="2Theta" unit="deg">
|
||
|
|
<startPosition>5.00547782</startPosition>
|
||
|
|
<endPosition>119.99571965</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Omega" unit="deg">
|
||
|
|
<startPosition>2.50273891</startPosition>
|
||
|
|
<endPosition>59.99785982</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Phi" unit="deg">
|
||
|
|
<commonPosition>0.0</commonPosition>
|
||
|
|
</positions>
|
||
|
|
<commonCountingTime unit="seconds">3.175</commonCountingTime>
|
||
|
|
<intensities unit="counts">86 75 87 96 87 88 81 69 72 73 99 83 88 87 92 83 86 84 93 93 89 80 98 86 86 81 84 84 94 103 115 87 89 95 87 77 77 93 95 80 112 94 92 94 93 82 84 73 120 96 92 101 94 98 89 88 75 100 84 103 103 81 88 104 92 89 103 83 76 113 94 100 104 106 106 101 82 77 88 71 90 87 94 105 87 88 94 84 99 93 95 95 84 80 89 104 95 99 78 92 90 96 84 94 112 103 113 78 98 77 83 100 116 113 107 96 104 104 110 86 105 63 88 96 106 93 126 92 111 84 100 96 86 110 98 80 110 99 80 104 95 111 111 94 81 111 104 80 89 87 93 103 64 104 78 93 106 93 116 86 112 89 101 109 92 111 105 100 107 93 105 105 103 113 88 95 132 110 124 109 89 105 96 120 86 112 111 118 87 133 105 103 101 103 96 90 104 118 110 110 121 96 95 92 110 88 103 120 96 98 92 112 115 109 88 103 116 111 104 110 110 103 101 155 100 103 99 113 99 107 100 107 113 103 124 107 116 129 104 101 107 106 141 126 113 123 113 113 86 105 113 105 117 103 109 111 121 112 117 107 121 95 111 121 109 99 107 110 112 116 107 118 115 116 127 104 120 120 113 118 123 120 101 106 127 121 109 118 109 116 116 105 118 105 122 133 117 122 134 105 130 143 106 121 117 104 113 93 103 126 113 110 113 101 88 121 143 124 127 110 122 110 104 104 135 128 105 100 101 94 120 116 117 115 110 112 122 133 111 109 118 118 117 117 111 130 126 113 139 107 126 109 139 100 116 135 120 141 123 104 124 113 124 123 133 138 112 135 117 121 120 110 117 140 157 132 116 120 126 128 146 120 115 111 112 124 113 118 133 122 111 109 127 124 116 138 136 109 127 112 134 123 136 110 128 147 118 139 136 133 111 126 117 112 127 126 104 136 112 115 139 117 123 138 112 141 129 135 135 116 120 146 134 122 122 134 129 144 124 124 127 117 129 134 150 116 146 117 138 124 127 134 126 146 109 106 145 138 129 130 126 139 146 146 129 104 141 98 136 127 127 124 163 149 136 140 144 128 147 116 139 135 110 135 118 132 149 151 132 138 135 147 143 98 130 145 141 132 128 144 149 144 164 138 143 129 157 133 150 121 150 135 146 136 167 156 150 153 149 133 132 129 123 133 136 143 121 150 130 141 145 130 167 136 160 160 121 136 126 156 150 144 130 126 127 134 141 146 134 123 150 139 133 132 138 152 146 138 133 174 136 161 155 132 149 134 153 140 135 187 160 155 129 130 138 146 127 166 157 167 146 164 138 151 161 134 191 160 158 141 133 146 143 130 129 150 152 139 133 136 149 143 163 146 170 152 140 139 156 140 147 147 169 145 126 127 143 145 152 152 161 147 185 164 163 149 151 176 160 172 150 126 183 156 149 133 181 134 163 135 146 122 144 147 150 143 179 156 151 129 175 168 147 162 121 141 160 163 176 122 135 151 157 168 146 152 133 147 151 155 162 156 161 161 169 139 163 130 150 155 146 156 157 144 141 149 153 123 183 155 153 181 146 149 152 151 147 189 152 172 176 175 163 152 170 172 161 163 140 172 175 166 155 151 168 172 144 189 152 169 144 151 143 146 162 168 158 158 164 155 185 157 173 145 174 146 185 175 158 168 178 169 158 156 155 158 140 167 185 152 164 155 170 173 162 172 153 139 168 173 162 167 164 181 167 150 129 173 187 173 192 179 179 151 167 172 175 161 149 170 175 164 178 166 162 191 190 189 170 180 158 172 180 168 144 172 163 153 157 163 162 169 185 139 191 162 176 153 153 175 187 169 169 169 173 152 166 161 166 181 170 156 190 179 169 152 160 157 189 185 180 180 183 184 176 158 152 145 167 146 151 157 184 179 179 160 162 170 190 184 147 195 180 181 170 179 186 158 166 141 172 190 193 163 196 173 167 195 169 157 183 176 170 184 183 164 180 163 169 173 169 155 158 172 179 173 151 166 168 184 169 207 185 149 202 180 191 198 195 151 173 187 180 144 164 186 160 151 172 189 187 179 178 163 179 169 184 186 169 156 204 174 169 185 207 181 184 191 195 185 225 152 160 172 208 173 162 195 175 168 176 160 164 172 168 161 209 151 191 180 198 181 214 158 162 185 218 208 192 203 184 166 172 204 210 206 170 187 160 216 168 189 183 186 174 172 197 168 174 166 174 167 175 208 170 195 220 225 166 201 221 170 181 170 202 175 184 181 183 175 201 215 175 174 189 161 196 210 187 172 215 192 168 193 196 185 204 174 195 166 183 181 200 189 180 195 206 203 183 207 202 200 163 179 181 186 170 189 174 220 157 202 215 185 183 178 185 178 197 200 198 166 1
|
||
|
|
</dataPoints>
|
||
|
|
</scan>
|
||
|
|
</xrdMeasurement>
|
||
|
|
</xrdMeasurements>
|