mirror of
https://asciireactor.com/otho/phy-4660.git
synced 2024-11-22 17:15:07 +00:00
109 lines
45 KiB
Plaintext
109 lines
45 KiB
Plaintext
|
<?xml version="1.0" encoding="UTF-8"?>
|
||
|
|
<xrdMeasurements xmlns="http://www.xrdml.com/XRDMeasurement/1.6" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.xrdml.com/XRDMeasurement/1.6 http://www.xrdml.com/XRDMeasurement/1.6/XRDMeasurement.xsd" status="Completed">
|
||
|
|
<comment>
|
||
|
|
<entry>Configuration=Reflection-transmission spinner, Owner=User-1, Creation date=11/29/2016 1:26:51 PM</entry>
|
||
|
|
<entry>Goniometer=Theta/Theta; Minimum step size 2Theta:0.0001; Minimum step size Omega:0.0001</entry>
|
||
|
|
<entry>Sample stage=Reflection-transmission spinner; Minimum step size Phi:0.1</entry>
|
||
|
|
<entry>Diffractometer system=EMPYREAN</entry>
|
||
|
|
<entry>Measurement program=C:\PANalytical\Data Collector\Programs\Burns Cu Spinner Gonio scan zero BH.xrdmp, Identifier={23998444-8D7A-4320-9B40-6587590B817D}</entry>
|
||
|
|
</comment>
|
||
|
|
<sample type="To be analyzed">
|
||
|
|
<id></id>
|
||
|
|
<name></name>
|
||
|
|
<preparedBy></preparedBy>
|
||
|
|
</sample>
|
||
|
|
<xrdMeasurement measurementType="Scan" status="Completed" sampleMode="Reflection">
|
||
|
|
<comment>
|
||
|
|
<entry>PHD Lower Level = 6.52 (keV), PHD Upper Level = 11.27 (keV)</entry>
|
||
|
|
</comment>
|
||
|
|
<usedWavelength intended="K-Alpha 1">
|
||
|
|
<kAlpha1 unit="Angstrom">1.5405980</kAlpha1>
|
||
|
|
<kAlpha2 unit="Angstrom">1.5444260</kAlpha2>
|
||
|
|
<kBeta unit="Angstrom">1.3922500</kBeta>
|
||
|
|
<ratioKAlpha2KAlpha1>0.5000</ratioKAlpha2KAlpha1>
|
||
|
|
</usedWavelength>
|
||
|
|
<incidentBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<xRayTube id="1010048" name="Empyrean Cu LFF HR (9430 033 7310x) DK410577">
|
||
|
|
<tension unit="kV">45.0</tension>
|
||
|
|
<current unit="mA">40.0</current>
|
||
|
|
<anodeMaterial>Cu</anodeMaterial>
|
||
|
|
<focus type="Line">
|
||
|
|
<length unit="mm">12.0</length>
|
||
|
|
<width unit="mm">0.4</width>
|
||
|
|
<takeOffAngle unit="deg">6.0</takeOffAngle>
|
||
|
|
</focus>
|
||
|
|
</xRayTube>
|
||
|
|
<sollerSlit id="21010002" name="Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<mask id="22080002" name="Fixed incident beam mask 10 mm">
|
||
|
|
<distanceToSample unit="mm">100.00</distanceToSample>
|
||
|
|
<width unit="mm">6.60</width>
|
||
|
|
</mask>
|
||
|
|
<antiScatterSlit id="22010003" name="Fixed slit 1°" xsi:type="fixedAntiScatterSlitType">
|
||
|
|
<height unit="mm">1.52</height>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<divergenceSlit id="22010012" name="Programmable divergence slit" xsi:type="automaticDivergenceSlitType">
|
||
|
|
<distanceToSample unit="mm">140.00</distanceToSample>
|
||
|
|
<irradiatedLength unit="mm">5.0</irradiatedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</divergenceSlit>
|
||
|
|
</incidentBeamPath>
|
||
|
|
<sampleMovement xsi:type="spinningSampleMovementType">
|
||
|
|
<spinnerRevolutionTime unit="seconds">2.0</spinnerRevolutionTime>
|
||
|
|
</sampleMovement>
|
||
|
|
<diffractedBeamPath>
|
||
|
|
<radius unit="mm">240.00</radius>
|
||
|
|
<antiScatterSlit id="22060009" name="Programmable anti-scatter slit" xsi:type="automaticAntiScatterSlitType">
|
||
|
|
<observedLength unit="mm">5.0</observedLength>
|
||
|
|
<offset unit="mm">0.00</offset>
|
||
|
|
</antiScatterSlit>
|
||
|
|
<sollerSlit id="21020003" name="Large Soller slits 0.04 rad.">
|
||
|
|
<opening unit="rad">0.0400</opening>
|
||
|
|
</sollerSlit>
|
||
|
|
<filter id="20010006" name="Beta-filter Rhodium">
|
||
|
|
<material>Rh</material>
|
||
|
|
<thickness unit="mm">0.050</thickness>
|
||
|
|
</filter>
|
||
|
|
<detector id="7010012" name="X'Celerator Scientific" xsi:type="rtmsDetectorType">
|
||
|
|
<phd>
|
||
|
|
<lowerLevel unit="%">40.5</lowerLevel>
|
||
|
|
<upperLevel unit="%">70.0</upperLevel>
|
||
|
|
</phd>
|
||
|
|
<mode>Scanning</mode>
|
||
|
|
<activeLength unit="deg">2.1223</activeLength>
|
||
|
|
</detector>
|
||
|
|
</diffractedBeamPath>
|
||
|
|
<scan appendNumber="0" mode="Continuous" scanAxis="Gonio" status="Completed">
|
||
|
|
<header>
|
||
|
|
<startTimeStamp>2017-03-30T15:55:32-04:00</startTimeStamp>
|
||
|
|
<endTimeStamp>2017-03-30T16:01:30-04:00</endTimeStamp>
|
||
|
|
<author>
|
||
|
|
<name>User</name>
|
||
|
|
</author>
|
||
|
|
<source>
|
||
|
|
<applicationSoftware version="5.4">Data Collector</applicationSoftware>
|
||
|
|
<instrumentControlSoftware version="7.9d 20161215">EMPYREAN</instrumentControlSoftware>
|
||
|
|
<instrumentID>0000000011187692</instrumentID>
|
||
|
|
</source>
|
||
|
|
</header>
|
||
|
|
<dataPoints>
|
||
|
|
<positions axis="2Theta" unit="deg">
|
||
|
|
<startPosition>5.00547782</startPosition>
|
||
|
|
<endPosition>119.99571965</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Omega" unit="deg">
|
||
|
|
<startPosition>2.50273891</startPosition>
|
||
|
|
<endPosition>59.99785982</endPosition>
|
||
|
|
</positions>
|
||
|
|
<positions axis="Phi" unit="deg">
|
||
|
|
<commonPosition>0.0</commonPosition>
|
||
|
|
</positions>
|
||
|
|
<commonCountingTime unit="seconds">3.175</commonCountingTime>
|
||
|
|
<intensities unit="counts">40 42 35 32 31 36 40 38 38 49 27 38 24 35 29 37 40 38 37 26 42 31 55 47 48 35 38 37 40 47 44 53 35 41 37 36 26 43 32 29 31 27 38 29 38 31 50 29 37 33 38 47 31 35 47 35 42 38 36 36 46 44 47 42 35 30 37 41 46 32 40 40 43 36 35 27 29 25 27 42 43 38 36 29 47 33 42 35 43 35 33 29 37 37 42 38 47 43 37 32 40 43 29 33 38 40 48 29 40 44 38 37 37 40 35 46 32 46 46 36 48 38 40 37 48 44 52 46 42 42 50 40 30 42 49 46 44 42 31 41 40 46 37 40 35 43 52 42 40 42 48 26 42 44 54 43 43 36 38 44 56 41 46 40 31 43 35 33 33 50 41 47 31 43 46 41 52 42 42 40 38 32 32 31 41 30 47 33 40 41 38 43 48 48 42 35 44 48 37 42 48 41 40 55 46 35 43 42 36 36 42 37 37 30 43 37 58 38 48 46 29 42 48 32 33 36 37 33 40 24 32 42 40 43 52 27 52 29 48 40 38 46 44 48 61 38 38 38 32 38 40 46 53 36 32 43 41 42 24 44 37 43 36 52 43 54 44 46 48 55 36 33 33 48 40 48 42 37 47 48 36 29 48 46 36 33 38 41 38 54 35 26 41 42 48 52 33 43 38 49 38 42 47 50 35 37 43 40 40 38 41 36 41 52 42 37 52 43 37 53 35 36 36 41 46 41 38 46 49 42 50 37 38 36 49 35 40 49 49 48 41 40 40 33 37 26 33 43 48 48 35 31 37 30 40 36 27 37 44 42 29 40 49 48 24 38 38 50 49 42 44 48 31 46 48 47 44 38 46 44 38 50 50 49 48 52 48 43 46 47 37 44 38 53 44 32 35 40 37 61 44 38 41 37 48 52 47 53 58 35 42 37 36 33 41 47 50 43 47 38 42 52 46 48 47 48 49 54 42 43 38 42 52 49 46 43 42 33 36 38 25 44 33 31 38 48 36 47 42 42 48 41 44 43 55 44 41 23 25 44 41 50 36 37 42 46 36 44 38 38 37 40 48 35 43 33 35 35 47 33 46 42 41 40 35 48 31 36 48 55 56 38 37 47 46 41 41 52 35 54 37 49 43 44 38 48 48 50 46 40 30 26 47 36 49 42 44 37 46 41 38 46 44 41 38 44 44 31 42 35 43 29 48 37 38 43 52 36 48 42 33 49 43 44 35 46 36 38 44 47 49 43 41 47 33 50 46 48 41 44 35 35 40 33 38 46 35 42 38 46 42 35 41 41 35 54 54 58 46 30 27 48 35 36 46 53 55 47 36 35 49 29 33 42 32 55 49 36 44 38 40 30 41 40 42 38 25 47 38 38 38 47 53 48 56 35 42 44 41 40 55 40 53 32 49 36 52 52 41 26 41 38 41 41 36 48 35 44 37 43 46 46 42 63 24 31 38 44 43 35 48 47 41 40 37 48 38 41 60 47 33 37 26 44 44 42 41 32 46 42 44 32 47 46 50 41 42 30 37 36 47 38 43 44 44 35 46 43 32 42 47 58 31 46 35 38 46 35 36 48 37 29 43 52 55 53 38 43 42 41 30 43 38 44 50 38 42 38 50 44 43 42 42 43 32 42 44 33 37 52 44 56 40 42 49 35 31 48 40 47 37 32 42 40 41 40 38 36 35 37 46 44 29 47 41 52 33 35 38 32 25 32 44 27 49 46 40 37 52 35 40 32 40 49 41 43 43 42 47 36 40 42 42 29 41 36 26 37 41 40 42 46 46 41 35 38 43 33 30 32 44 43 46 33 46 36 46 44 54 44 56 37 42 49 44 40 42 37 50 50 44 38 29 44 52 40 36 46 36 43 46 46 36 40 44 42 35 44 35 24 47 44 43 44 42 32 55 46 48 48 32 38 41 40 47 33 35 32 30 26 46 42 37 38 36 32 26 42 50 42 25 35 33 48 37 33 38 42 35 52 29 38 46 48 40 41 32 36 37 48 43 43 41 33 49 47 33 31 50 37 56 43 33 46 58 27 37 48 38 41 31 40 46 43 56 35 41 35 36 44 26 54 41 47 35 30 42 33 32 29 44 35 44 37 36 37 44 41 40 44 36 26 35 38 41 27 49 44 35 48 40 27 40 42 35 44 47 36 43 33 48 48 36 33 42 37 54 43 30 37 33 49 40 29 40 36 41 33 36 43 25 33 44 53 43 37 63 46 31 37 30 53 52 55 41 33 41 44 60 41 36 50 36 41 43 35 47 31 44 37 35 33 43 32 44 38 40 50 42 40 54 31 49 46 46 42 41 37 38 38 43 36 30 33 27 37 40 36 48 33 52 38 41 38 48 59 36 49 44 38 50 26 33 38 32 46 38 33 33 40 38 37 36 44 44 31 35 42 33 36 42 43 44 49 41 37 46 30 40 36 49 33 27 47 37 42 38 49 30 49 42 35 48 48 40 47 27 35 31 35 44 42 32 47 37 41 37 53 48 46 41 32 40 46 37 47 40 38 38 41 36 47 37 38 43 38 38 42 36 29 43 31 43 29 46 37 33 35 37 33 37 37 26 32 38 38 40 38 40 36 35 52 37 38 24 30 31 35 35 37 35 50 44 37 42 49 40 53 29 44 47 36 49 49 29 31 24 42 27 32 35 33 55 37 30 40 42 46 32 46 50 33 30 36 35 30 40 47 35 40 41 37 19 44 26 32 43 43 35 38 44 29 38 30 32 33 40 38 40 38 30 38 23 46 37 38 25 48 48 35 44 47 25 46 35 44 43 33 35 41 37 41 49 44 33 36 40 50 31 41 36 37 24 26 36 33 32 43 40 53 32 30 35 35 36 37 41 43 43 41 43 41 41 35 44 47 38 37 47 43 29 43 30 41 25 35 44 49 41 38 58 30 30 44 50 31 40 31 27 40 33 26 32 35 36 40 36 27 40 31 53 41 43 25 27 31 42 36 40 35 40 41 41 33 37 35 43 37 36 40 55 31 33 38 30 46 40 42 33 29 47 44 50 36 41 23 35 37 35 42 21 36 41 43 43
|
||
|
|
</dataPoints>
|
||
|
|
</scan>
|
||
|
|
</xrdMeasurement>
|
||
|
|
</xrdMeasurements>
|